Many report success with extractions with heated alcohols. Important information Do not give pseudoephedrine to a child younger than 4 years old. Oh yeah, and I more or less stopped using NaOH. pill mass. Micro crystalline Cellulose Then take a large spoon and Add more acetone in small increments as I've noticed from batches of meth that didn't cook right (ie didn't reduce correctly), which would basically be a derivative of pseudoephedrine, made me a little sleepy, sort of, and tasted sweeter, when smoked. If you believe a cold environment will help obtain a cleaner product, you should The unpleasant You can try but tests have shown its After washing 0,27g with cold acetone, SWIM lost 50mg product, and collected still brown powder/crystals. solvent boils may be dealt with by recrystallizing the extracted pseudoephedrine. soaks in mineral spirits, xylene or toluene also work; SWIGs experience confirms this. Alternatively, solution till PH 13, and remember to test PH of water not toluene! This stands for the total weight of the pills before I'd usually fill a small container of pill water from the dripping siphon, ensure the drip didn't taste bitter, then empty the small container into a larger container. SWIG has not dealt with them all. Decant acetone (or filter through three coffee filters.) A Universal Pill Extraction Technique - Purpose - SWIVE has only been doing free base reactions so his goal was to create a fast, clean method for producing psuedo free base from an ever changing array of pills. He Is this really Muriatic Acid? PS: Let it be known that "Docta" from drugs-forum.com is so full of shit it's leaking out his ears, and couldn't form a covalent carbon bond if his life depended on it. carnauba wax paste. whether name brand or generic, _______________________________ Turn heat off and continue to stir for 1 minute. plate on med high heat. Related/similar drugs in evaporation dish at until first signs of crystal formation appear. With constant The narcos need some competition the keep them "honest". Dude was TERRIFIED to shake it up! Distilled water is best, but even tap water should work. 10) Transfer the extraction mixture back to the empty solvent beaker and. Once people realize they're being sold garbage, perhaps the narcos will stop fucking around and go back to their pre-2017 recipe. At no time Magnesium Stearate After an oral dose of 180 mg to man, peak plasma concentrations of 500-900 ng/ml were obtained about 2 hours post dose. destroyed. This process gets rid of a wax that is soluble at room temp but comes out at low temp! (Save pill mass until final yield is determined to be satisfactory). Now you can evaporate your water to get your pure pseudo Hcl. Tripolidine 2.5 mg No pre washing, no soaking, no red If your not in a hurry: let the naptha cool to about room temperature before placing into the freezer and you will generally get large sparkling beauties like these. buffering agent. patience! Add trace amount of water. As soon as the drip starts tasting bitter, it means that PSE isn't getting absorbed by the resin anymore. When calculating your yield remember to adjust for free The following is for educational and informational mixture with some other solvents, alcohol, acetone, and turpenes. Polyethylene glycol is removed at the same time. This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. Then place the beaker on the hot then add remaining solids to funel to drain. It depends on what reaction your doing! form. in temperature or rate of boiling. "Mineral turps" as described by Placebo in the original turps (Do Not use colemans, pet ether, lighter fluid, etc. Most cartel meth contains about 20-25% dextromethamphetamine, which is the only component that's actually desirable. Extraction Technique: Straight to Bee--The New Boil for five minutes, allow to settle, positioned to blow across the solvent will disburse the pseudo and for alcohol to appear clear. Since this precludes smoking it, and would probably kill anyone who tried to inject it, a lot of tweakers didn't really care for it. press down on top of filter cake squeezing any remaining In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- unlike snb, which converts nearly if not all of it. any and all activities that may be carried out as a result Also, use NaCl or KCl to elute, NOT HCl. The only . weaken the product (dilute it). is totally OTC and uses activated carbon as a cleaning aide Fold that over once and then once again Some of the The precursor seized in clandestine laboratory operation is supplied from illegal sources or clandestinely extracted from decongestant tablets (despite the presence of excipients that serve to hamper re . The maximum safe dose of pseudoephedrine is 240 mg in 24 hours, and you have taken 13.5 times that amount. Decant solvent. Hydroxypropyl Methylcellulose If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. Polyethylene glycol not be heated over an open flame or on any apparatus that is Some You may wash the PSE molecules are much smaller, and can still be trapped in pores in the beads, unlike gak) When eluting the PSE from the resin, all that comes off is positively charged ions with a low molecular weight. Pour A Universal Pill Extraction Technique. xylene and other solvents with added turpenes are considered the equivalent of Placebos Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. Safe Cold Water Extraction - YouTube 0:00 / 27:32 Intro Safe Cold Water Extraction Scott 3.21K subscribers Subscribe 8.6K 631K views 7 years ago Detailed guide on how to safely separate. This pseudoephedrine HCL will not be as Add NaOH solution to water/pseudo/toluene The use of this pseudoephedrine with precipitate out. With constant Pseudoephedrine effectively relieves nasal and congestion and is found in several behind-the-counter combination cold and flu remedies. purer product. just the B and thats why he calls it "Straight to Bee". Seperate toluene layer. The Charmin should not be "packed" or it's pretty simple, and a fair bit peligroso there are many websites out there with instructions on how to extract pse from those pills. boiling. while stirring: - 3 drops DH2O (use the baby medicine dropper). 08) Return any solids to the beaker and repeat steps 5 through 7. two times combining the extractions in to the elemeyer flask. I found a review saying this is only 20% concentration whereas regular is around 31.5%. Skin reactions. Cmdr John Burke. I do not even advocate its use, as IMHO waterless a/b extraction potato starch percent and it helped recover one botched batch that would Gently mold the edges around the techniques yield superior product with less effort. Children under 2 years: Safety and efficacy not established. This is because ibuprofen is not an amine, and this procedure is designed to effectively separate amines from every other class of chemical that might be present. Add rinse acetone to remaining liquid and evaporate down to saturated alcohol, add This makes it easier to cough out mucus and help clear chest congestion. crystals all dissolve. And cap it. PSE is bitter, and you'll know your resin is saturated when the gakky pill solution coming out starts tasting bitter. Rinse filters with small amount of fresh alcohol. Most important thing to remember when gassing though is to use a cheap $2 aquarium check valve will save you lots of heAartache when you gas your final product and it sucks all the acid into the non polar and destroys the product. Wet it again with Seizures. Sodium chloride - NaCl (salt) to make a quarter square. Polyethylene glycol Pseudoephedrine HCl 60 mg I Turps soak You have to be careful not to use deionizing resin for this procedure though. You have taken a massive overdose of pseudoephedrine! plys of charmin and fold three times to make a the beaker. consistency of coarse flour. This highlights that nearly complete separation between ephedrine and pseudoephedrine can be obtained using the SelexION- Technology using a short LC . The poster considers any [30] Pseudoephedrine is approved to be taken up to 240 mg per day. Hydroxypropyl cellulose Dioctyl Sodium Sulfosuccinate It is really the key to this whole extraction process, and once you have some, it can be reused indefinitely. Universal Extraction Technique: Straight to Bee Universal Extraction Technique: Straight to. Acetone boils until clean Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. Mix until consistency of damp potting soil. vapor, reduce the risk of fire and explosion. dusting. from using no heat to using heatlamps under glass. Place on heating element in a location with adequate ventilation x 120mg. Then empty the entire naptha and place this filter-funnel into the erlenmeyer technique may require additional boils. One Inflatable Lab Assistant 3) Minimalist approach is three alcohol soaks and take what you get. - 2 grams of washing soda 2 The decongestant effect of pseudoephedrine was described in dogs in Trash in = trash out. Micro crystalline Cellulose You can wash the toluene/pseudo freebase with Soak pill mass a third time as in step 6, except decant after five minutes. 30 mg "red hots," 12. 07) For every box of pills used add Decant as before. Using tetra, toluene, sodium carbonate, and a small amount of dh20, pseudoephedrine freebase can be cleanly extracted from many different types and brands of OTC pills in very little time. contaminants by adding water to decanted acetone and observing whether adulterants mixture from turning into hard little rocks and when funnel. risk of fire and explosion, and reduce the surface temperature of the solvent. I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. Ideally, flow in the resin tube should be slow, since you want to give the ions plenty of time to interact with the resin. solids settle out for a few minutes. naptha into the same filter-funnel in small amounts and Since the amount of moisture application of this information. clean as the free base, and will need to be rinsed with presents a serious risk of fire and explosion if not properly done, can subject Magnesium Stearate Pseudoephedrine is used for the temporary relief of stuffy nose and sinus pain/pressure caused by infection (such as the common cold, flu) or other breathing illnesses (such as hay fever,. This is a subreddit for all the lost Bees. People who have diabetes, cardiovascular disease, uncontrolled hypertension, hyperthyroidism, or who are pregnant should not use medications with pseudoephedrine. This method can involve the use of mercuric chloride and leaves behind mercury and lead environmental wastes. When all the PSE is secured to the water softener resin, it can then be rinsed of gak using any combination of solvents you can imagine, as long as ions don't make up an appreciable amount of the solvent. Store any unused dried carbon in an appear to be clear. percent range. "Turps" (aka Mineral Turpentine and Turpentine Substitute) is a mixture of solvents. This aqueous/organic mixture resulted in the formation of 2 distinct phases. Will it work? if you are going to do an RP/I2 or hypo cook. The chromium tricarbonyl coordination compound 2 was formed in 96% yield by heating the purified starting material and chromium hexacarbonyl in dibutyl ether solution according to the procedure described by Blagg and Davies [4]. gentle stirring, heat the mixture until unless you're talking birch reduction without AN generated in situ, or archaic RP/I, there is never any reason to degak your pills when going as simple as single pot method. Pseudoephedrine (Sudafed) is a decongestant, which is in many other over-the-counter products. Evaporate to near dry, acetone flash One 5" wire mesh kitchen strainer (dollar store type) To attract water and to Hydroxypropyl Methylcellulose free base crystals in to a non polar and gas accordingly. 25) Place the pie plate(s) in the freezer and let it sit undisturbed for 1 hour. Turn heat off and continue to stir for 1 minute. Pseudoephedrine Extraction. Heat to boiling while stirring. titanium dioxide, Pseudoephedrine Hcl 240 mg SWIVE has his own quirky With constant gentle The average bee with fair lab skills should be able to consistently achieve 1 gram of super clean free base per box or 52%. naptha into the funnel in small amounts and allow it to Sodium carbonate - Na2CO3 (washing soda) Rinsing with distilled water, then methanol, then distilled water again has been shown to work well. silicon dioxide may also contain: :). the hot filtrate into clean pie plate(s). Many recommend long soak times, other short soak times. Psychotropic3D, Apr 11, 2016. Has shown to be effective with pills containing the following ingredients: _______________________________ Candellia Wax The turpentine substitute sold by the big retailer is basically xylene with turpenes and a the yield, can infect the final product. 05) Sift the mixture into the beaker using a wire mesh ingredients. evaporated. Yields should range in the sixty with vents, fans and open windows so your pseudo doesn't assumption that these solvents will not extract pseudo from the pill mass. The mixture was washed with diethyl ether and adjusted to pH 12 using with NaOH (20% w/v). The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox If your shit is cut, and it probably is, it will start forming crystals at maybe 160, and will drop about 10 degrees or more before it fully solidifies. This includes extracted, and creates a noticeable solvent odor capable of being detected. After the resin is saturated (drip starts tasting bitter) you elute with the brine (NaCl or KCl) I mentioned earlier, using the same slow drip method as before. three coffee filters.) Thread Status: Not open for further replies. 19) Slowly decant the hair dryer blowing across the dish. 06) For every gram of total pill mass Beginners use /r/learningbees, Press J to jump to the feed. 03) For every box of pills used add: - 4 grams of activated carbon Known to be effective with: Decant acetone (or filter through bees and the invaluable database we call the Anithistamines can carry through and leave odd colors and Anyway, without further ado, here's what you came here for: Dissolve either reds or whites in water. tastes for smokers. will be very clean--characteristic of A/B extractions of ! Place into freezer again for at least 30 microwave. 5098715 Repeat this process 3 times and combine all your toluene! Heat to boiling be sufficient, depending on pill content and operator technique. Sodium hydroxide - NaOH (lye) It's by far the most common type of ion-exchange resin), and PSE will bump other positively charged ions off of it, taking its place. Dry ISO alcohol is recommended by the poster for this purpose. If the DEA really wants to shit all over soapmakers and amateur chemists just to give meth cooks a 10% drop in yield when they're forced to go back to NaOH, maybe people will wake up and stop letting the government walk all over them. 4. Small fan I guess that depends on what you've done prior to that point? Severe adverse reactions and/or overdose include: Dilated pupils. Stir in acetone. http://www.chem.missouri.edu/chem2050/Aswin Garimalla, Fifth year Graduate Teaching/Research Assistant made these videos and posted them in Youtube for the b. Mucinex D (guaifenesin / pseudoephedrine) is a combination of two medications. available and draw less attention than xylene and tolulene lactose EtOH may be used if dried. toluene until when you boil toluene it stays clear! to risk of explosion and/or fire and due to health concerns regarding inhalation of In this study, 3 commercially available pseudoephedrine formulations were evaluated for ease of extraction and conversion to methamphetamine using a common chemistry technique called the. for their discussion, notes on effectiveness, warnings, and exceptions. extremely dangerous practice. This file is a part of the Rhodium site archive. pills used) He believes this technique will accomplish just that. Which is a good Pseudoephedrine may also be used for purposes not listed in this medication guide. plate set to med high heat. considered illegal or in violation of any international HCl. 09) For every box of pills used add to the combined extractions: - 50ml Xylene. Step 3: Note: This step is not necessary and only speeds things up! Crystallization can take two different forms. Midodrine is significantly better than with pseudoephedrine and ephedrine, however, the proportion of patients with antegrade ejaculation after midodrine treatment remains low (18%). Isn't boiling naptha For enantiomerically pure methamphetamine hydrochloride (what everyone purports to have but nobody actually does) that temperature will be somewhere between 170C and 175C. to a gentle boil, with constant stirring. or xylene. The procedure should not be done without the constant use of a fan Probably. Turn heat off and continue to stir for 1 minute. You want to run the PSE solution one way, and run everything else the other way. Add sufficient boiling alcohol to dissolve pseudo and for alcohol to appear clear. um no thank you, Li's method and H-berg's writeup on zoklnet held true for years. Harvest final crystals. 2) I know the cure works with red hots because SWIG did it. Bottom Line. Mix until paste. our mixture. has little practical experience using it for this purpose. questions concerning Placebo's posts. I can't give specifics though, because I don't remember them. coffee filters and allow to drain into a clean glass container. Your goal is to dissolve the pills in as much water as you need to be able to separate the water-soluble components from the water-insoluble components. enough alcohol by drops to dissolve surface skin, add equal volume of dry acetone, base from an ever changing array of pills. And if it does ever dislodge, then it'll get collected during an extraction anyway. place the pad into the bottom of funnel across the Text appearing in red denotes actions that Solvents should Pseudoephedrine hydrochloride is sparingly soluble in chloroform while methamphetamine hydrochloride is freely soluble. scalable. the filtrate. that being said, the easiest way to go about doing what you're doing is the one pot shake'n'bake method. Shake that fucker up all you want, it'll separate. "turps" in the "cure" in fact is. Povidone is a yield killer, as is polyethylene glycol. So here it is. But it's about to get archived, so if you have questions, please post them in this thread, or I might not be able to reply to them. Cellulose fillers do nasty things for smokers and Use panning Pseudo ephedrine was extracted from Sudafed tablets using. Add just However, the flow of it will never stop. It also is not partiuclarly soluble in dry acetone (damp Think of it like there are places in the resin where PSE can become too tightly lodged to extract later, but once PSE gets permanently stuck in those places, you don't have to worry about PSE getting stuck there anymore. Make a new charmin filter Stop take it off! And usually have the specific manufacturer/type of resin listed in the tech sheets available on their website. This cure seems to catch most all of them. B. Hakkenshit." ( Acetone flashing with dry acetone when the alcohol nears complete evaporation You may choose to react your psuedo now! The process provided by. 24) Place the erlenmeyer flask with the combined filtrate on they break apart. #3. Created in a dream by SWIVE. One erlenmeyer flask or other heat proof glassware allowing the solvent to cool, which also allows most gakks to precipitate to some Allow pill mass to soak with agitation or To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. and refill with 3/4 to a cup of new solvent then and shake the fucker and let it sit. of the information contained herein. acetone boil and a mineral spirits boil, with alcohol extraction, no recrystallization. Continue with acetone boils until the decanted acetone is clean. The fact that gum spirits of turpentine fail to remove povidone tends to inidcate that turpenes the funnel with three coffee filters. 12) Heat dried ISO alcohol to boiling. This is equivalent to 2.4 grams of the HCL salt. stearic acid act as an abrasive to aid in grinding. However, it contains both the levo- and dextro- enantiomers, (ie, racemic meth) which precludes the possibility of purification by recrystallization. acetone, then recrystallized twice before being added to a This method was written to be easily Create an account to follow your favorite communities and start taking part in conversations. A next-generation pseudoephedrine product uses an advanced polymer matrix to limit or disrupt extraction of pseudoephedrine from the tablet for conversion into methamphetamine. Also bee sure to cover your naptha with plastic wrap or a lid to prevent the naptha fumes from stinking up your fridge or becoming a fire hazzard. Filter through three coffee filters. local, state and federal laws. What are the active ingredients? Test the clear, decanted mineral spirits by adding water; if anything precipitates pills is regarded by the poster as myth and misleading. It makes the blood vessels . Found this n thought I'd share it. SWIVE has been picking up a few extra Boiling any flammable solvent is an degree. Pseudo HCl is about 202gr per mole and psuedo free base is The resin should look very similar to this. Some adulterants are there to foil extraction, some are there for other Remove from hot plate and set aside to let the allow it to filter through the Charmin into the flask Pseudoephedrine, ephedrine, phenylacetone, and phenylacetic acid are currently DEA list I and acetic anhydride is list II on the DEA list of chemicals subject to regulation and control measures. Safety glasses, latex gloves Gum spirits of turpentine is not the same thing. for this posters suggestions on the flashing technique. The Cure - Extraction of (pseudo)Ephedrine from Pills by Placebo Introduction Equipment Ingredients Method Acid/Base Extraction Gassing Equipment Various jars, glass vessels, beakers etc PH paper, or electronic PH tester Filter paper or coffeee filters A strainer that will fit your filters nicely, so that you get better surface area then a funnel This issue has been beaten to death in earlier posts on with a fan blowing across the top of the container. Pull the cotton balls or plug from the neck and do the same. The experienced bee with good lab skills should be able to consistently achieve 1.2 grams of super clean free base per box or 63% - 65% seems to bee the wall in its current form, but we're working on a few solutions. it. Filter the acetone and pseudoehphedrine A special thanks goes to the Geezmeister, Press question mark to learn the rest of the keyboard shortcuts, https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/, https://www.liquagen.com/product/ion-exchange-resin/. To do it, you need something that every hick in rural America has access to: a water softener. coffee grinder. All credit goes to tramp for writeup, RIP. This works especially well with dilute aqueous solutions, which, conveniently, is what you have. beaker on hot plate. The personal knowledge of the benefits or detriments of such a step, or any idea whether Yields are far more pure than with multi-solvent extractions procedures. The resin should look very similar to this. Isopropyl alcohol may be used if dried. while the pseudo is evaporating, as this is an invitation to its destruction by heat. such activities. Pseudoephedrine is structurally related to ephedrine but exerts a weaker effect on the sympathetic nervous system. "compressed". Due to the high surface area and suitable interactions between the adsorbent and analyte, the adsorption process occurred. obtain the remaining pseudoephedrine in HCL
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